Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | 1,4-Dioxane | HCID 31275 | — |
| Edukt | 5-Nitro-2-thenoic acid | HCID 80591 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Ethyl 5-nitrothiophene-2-carboxylate | HCID 304627 | — |
Reaktionsschritte
5 g of 5-nitrothiophene-2-carboxylic acid was stirred in 100 ml of ethanol. 20 ml of dioxane containing 4 M of hydrogen chloride was added to the obtained mixture, and they were stirred at 60° C. for 2 days. The solvent was evaporated to obtain the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US06710056B2 |
|---|
| Quelldatensatz | uspto-grants-2004_03 |
|---|
| ORD ID | ord-f84d5a426a894c01af94fb8ebc136096 |
|---|
| Quellennotiz | uspto-grants-2004_03 |
|---|
