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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 500327Erstellt: 25. Oktober 2026

Benzyl Bromide → 1-Benzyl-N-tert-butylcyclopropane-1-sulfonamide

https://huagongshe.com/reaction/500327

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzyl BromideHCID 7498—
EduktEthyl AcetateHCID 8857—
EduktN-tert-butyl-1-methylcyclopropane-1-sulfonamideHCID 21889792—
LösungsmittelHexaneHCID 8058—
Produkt1-Benzyl-N-tert-butylcyclopropane-1-sulfonamideHCID 2188979660%

Reaktionsschritte

This compound was obtained in 60% yield using the procedure described for the synthesis of N-tert-butyl-(1-methyl)cyclopropylsulfonamide except 1.05 equivalents of benzyl bromide were used, followed by trituration with 10% ethyl acetate in hexane: 1H NMR (CDCl3) δ 0.92 (m, 2H), 1.36 (m, 2H), 1.43 (s, 9H), 3.25 (s, 2H), 4.62 (br s, 1H), 7.29-7.36 (m, 5H).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07772180B2
Quelldatensatzuspto-grants-2010_08
ORD IDord-c98f49bca4274f19ba2f91084d747ef4
Quellennotizuspto-grants-2010_08