HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 503022Erstellt: 27. Oktober 2026
Methanol → Hexanoic acid, 2-methyl-, methyl ester
https://huagongshe.com/reaction/503022
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Methanol | HCID 887 | — |
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | 2-Methylhexanoic Acid | HCID 20653 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Hexanoic acid, 2-methyl-, methyl ester | HCID 519892 | 93% |
Reaktionsschritte
A solution of 2-methylhexanoic acid (20 g, 153 mmol) in methanol (500 mL) was treated with concentrated sulfuric acid (8.0 mL) and heated to 50° C. for 16 h. The reaction was diluted with water and extracted with ether. The combined organic layers were dried and concentrated to afford 20.57 g (93%) of methyl 2-methylhexanoate as a colorless liquid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US07776896B2 |
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| Quelldatensatz | uspto-grants-2010_08 |
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| ORD ID | ord-dd7c0667478e4394b22e5f59ab7fce31 |
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| Quellennotiz | uspto-grants-2010_08 |
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