HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 50520Erstellt: 25. Oktober 2026
2,5-Dinitrophenol → 1-Bromo-4-(2,5-dinitrophenyloxy)but-2-ene
https://huagongshe.com/reaction/50520
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 2,5-Dinitrophenol | HCID 9492 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 2-Butene, 1,4-dibromo- | HCID 13180 | — |
| Lösungsmittel | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Produkt | 1-Bromo-4-(2,5-dinitrophenyloxy)but-2-ene | HCID 73994035 | — |
Reaktionsschritte
A mixture of 2,5-dinitrophenol (4.0 g), potassium carbonate (4.6 g), NMP (40 mL) and 1,4-dibromo-2-butene (14.0 g) is heated to 45° C. for 2 hr. Extraction in the normal fashion and Kugelrohr distillation of the excess dibromide (0.1 mm Hg, 80° C.) gives 1-bromo-4-(2,5-dinitrophenyloxy)but-2-ene (mp 81-83° C.).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US06713135B2 |
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| Quelldatensatz | uspto-grants-2004_03 |
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| ORD ID | ord-f5e80ea4bce44aebb9b6189df4f7579d |
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| Quellennotiz | uspto-grants-2004_03 |
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