HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-((Trifluoromethyl)thio)aniline → 2-[4-(dimethylamino)phenyl]-N-{4-[(trifluoromethyl)thio]phenyl}acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-((Trifluoromethyl)thio)aniline | HCID 123054 | — |
| Edukt | 4-N,N-dimethylaminophenylacetic acid | HCID 152203 | — |
| Produkt | 2-[4-(dimethylamino)phenyl]-N-{4-[(trifluoromethyl)thio]phenyl}acetamide | HCID 44243115 | — |
Reaktionsschritte
The product was prepared from 2-(4-(dimethylamino)phenyl)acetic acid (23 mg) and 4-trifluoromethylthioaniline (28 mg) according to Method C: 1H NMR (300 MHz, CDCl3) δ ppm 2.98 (s, 6 H), 3.66 (s, 2 H), 6.72-6.78 (m, 2 H), 7.14-7.19 (m, 2 H), 7.19 (s, 1 H), 7.43-7.51 (m, 2 H), 7.52-7.57 (m, 2 H); MS (ESI-pos) m/z 355.0 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07786171B2 |
| Quelldatensatz | uspto-grants-2010_08 |
| ORD ID | ord-f7b001fe97a5435f810370dd53f80a26 |
| Quellennotiz | uspto-grants-2010_08 |