HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Hexanol → 2-Hexyl methanesulfonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Hexanol | HCID 12297 | — |
| Edukt | Methanesulfonyl chloride | HCID 31297 | — |
| Produkt | 2-Hexyl methanesulfonate | HCID 15369440 | — |
Reaktionsschritte
The title compound was prepared by following the general procedure of Example 43 for mesylation as a colorless oil (408 mg, 68%) from 2-hexanol (312 mg, 2.90 mmol) and methanesulfonyl chloride (500 mg, 4.40 mmol). 1H NMR (CDCl3, 300 MHz) δ0.89-0.94 (m, 3H), 1.31-1.43 (m, 5H), 1.57-1.71 (m, 4H), 2.99 (s, 3H), 4.76-4.82 (m, 1H) ppm.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06713471B1 |
| Quelldatensatz | uspto-grants-2004_03 |
| ORD ID | ord-59f6081212b546948c3be8343fc3cd12 |
| Quellennotiz | uspto-grants-2004_03 |