7-(4-hydroxybut-1-ynyl)-9,9-dimethyl-9H-fluoren-2-ol → 7-(4-Hydroxybutyl)-9,9-dimethyl-9H-fluoren-2-ol
Reaktionsgleichung
[OH:1][CH2:2][CH2:3][C:4]#[C:5][C:6]1[CH:18]=[C:17]2[C:9]([C:10]3[CH:11]=[CH:12][C:13]([OH:21])=[CH:14][C:15]=3[C:16]2([CH3:20])[CH3:19])=[CH:8][CH:7]=1>C1COCC1>[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][C:6]1[CH:18]=[C:17]2[C:9]([C:10]3[CH:11]=[CH:12][C:13]([OH:21])=[CH:14][C:15]=3[C:16]2([CH3:19])[CH3:20])=[CH:8][CH:7]=1Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
7-(4-Hydroxybut-1-ynyl)-9,9-dimethyl-9H-fluoren-2-ol is hydrogenated to completion in THF on palladium/active carbon. The catalyst is filtered off, the solvent is removed in vacuo, and the residue is employed in the next step without further purification.
Aufarbeitung
- filtrationThe catalyst is filtered off
- customthe solvent is removed in vacuo
- custom