HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diethyl(4-nitrophenyl)phosphonate → P-(4-Nitrophenyl)phosphonic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diethyl(4-nitrophenyl)phosphonate | HCID 284865 | — |
| Lösungsmittel | Hydrochloric Acid | HCID 313 | — |
| Produkt | P-(4-Nitrophenyl)phosphonic acid | HCID 196997 | 100% |
Reaktionsschritte
A solution of diethyl (4-nitrophenyl)phosphonate (60 g, 230 mmol) in 250 mL of concentrated HCl (aq) was stirred at reflux overnight. The excess HCl was removed under reduced pressure and the product used in further chemistries without purification (46.8 g, yield: 100%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09096624B2 |
| Quelldatensatz | uspto-grants-2015_08 |
| ORD ID | ord-00ef7beb8b9644988eeff1d44a1fe193 |
| Quellennotiz | uspto-grants-2015_08 |