HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Thiophenecarboxaldehyde → HCID 178424285, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Thiophenecarboxaldehyde | HCID 7364 | — |
| Edukt | Benzoyl chloride, 3,4-dichloro- | HCID 76403 | — |
| Edukt | Fmoc-leucine | HCID 1549133 | — |
| Edukt | HCID 178523876 | HCID 178523876 | — |
| Produkt | HCID 178424285 | HCID 178424285 | — |
Reaktionsschritte
Following the procedure of Example 28(a)-28(d), except beginning with Wang bound Fmoc-L-histidine (Trt) instead of Wang bound Fmoc-L-leucine, and substituting furan-2-carboxaldehyde for thiophene-2-carboxaldehyde, and substituting o-toluoyl chloride for 3,4-dichlorobenzoyl chloride, the title compound was prepared as a solid. MS [M+H]+424.4
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06713502B2 |
| Quelldatensatz | uspto-grants-2004_03 |
| ORD ID | ord-a496ed6aec304f68915dfbe7dd5050ff |
| Quellennotiz | uspto-grants-2004_03 |