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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 51210Erstellt: 25. Oktober 2026

N,N-Dibutylaniline → 5-Butoxy-4-methyl-1,3-oxazole

https://huagongshe.com/reaction/51210

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN,N-DibutylanilineHCID 61154—
Eduktn-Butyl alpha-isocyanopropionateHCID 11171108—
Produkt5-Butoxy-4-methyl-1,3-oxazoleHCID 987744098,7%

Reaktionsschritte

Example 5 is repeated except that a mixture of 11.8% by weight of n-butyl α-isocyanopropionate and 88.2% by weight of N,N-dibutylaniline is added continuously via the inlet (A). 4-Methyl-5-n-butoxyoxazole is obtained in a yield of 98.7% via the top takeoff B and the amine via the sidestream takeoff D.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06713630B2
Quelldatensatzuspto-grants-2004_03
ORD IDord-2e9a3f31681747fb86ec406eef7c2bbf
Quellennotizuspto-grants-2004_03