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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 514338Erstellt: 25. Oktober 2026

Hydrochloric Acid → 2-Hydrazinylpyridine-4-carbonitrile hydrochloride salt

https://huagongshe.com/reaction/514338

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrochloric AcidHCID 313—
Edukt2-Hydrazinylpyridine-4-carbonitrileHCID 20118714—
LösungsmittelEthyl AcetateHCID 8857—
Produkt2-Hydrazinylpyridine-4-carbonitrile hydrochloride saltHCID 8672548495%

Reaktionsschritte

To a solution of 2-hydrazinylpyridine-4-carbonitrile (2.13 g, 16 mmol, PREPARATION 2) in EtOAc (10 mL) was added HCl (4 M in EtOAc, 15 mL) at rt. It was then stirred at rt for 30 min. The reaction mixture was filtered and washed with EtOAc and dried to give the title compound (3.13 g, 95%) as a yellow solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09107916B2
Quelldatensatzuspto-grants-2015_08
ORD IDord-a78809a1a8e44a92b3a4ade8149e844e
Quellennotizuspto-grants-2015_08