3-Methylacetophenone → (2E)-3-(Dimethylamino)-1-(3-methylphenyl)prop-2-en-1-one

Beteiligte Stoffe

Reaktionsschritte

The title compound was prepared in 35% yield from 1-(3-methylphenyl)ethanone and DMF-DMA according to the procedure for the preparation of Example 12, part A. 1H NMR (400 MHz, CDCl3): δ 2.39 (3H, s), 2.79-3.11 (6H, m), 5.70 (1H, d, J=12.4 Hz), 7.24-7.31 (2H, m), 7.66-7.71 (2H, m), 7.78 (1H, d, J=12.4 Hz).

Herkunft & Nachweise