cis-7-Methoxy-1,2,3,4,4a,5,6,10b-octahydrobenzo[f]quinoline → HCID 178488316, Verbindung
Reaktionsgleichung
[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([OH:12])=O)=[CH:9][C:4]=2[N:3]=[CH:2]1.[CH3:13][O:14][C:15]1[C:28]2[CH2:27][CH2:26][C@H:25]3[C@H:20]([CH2:21][CH2:22][CH2:23][NH:24]3)[C:19]=2[CH:18]=[CH:17][CH:16]=1>>[NH:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10]([N:24]3[C@@H:25]4[C@@H:20]([C:19]5[CH:18]=[CH:17][CH:16]=[C:15]([O:14][CH3:13])[C:28]=5[CH2:27][CH2:26]4)[CH2:21][CH2:22][CH2:23]3)=[O:12])=[CH:9][C:4]=2[N:3]=[CH:2]1Komponenten
3
Versuchsvorschrift
The title compound is prepared from 1H-benzoimidazole-5-carboxylic acid and cis-7-methoxy-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline following a procedure analogous to that described in Example 1. Yield: 85% of theory; LC (method 1): tR=2.62 min; Mass spectrum (ESI+): m/z=362 [M+H]+.
Quellen und Nachweise
- ORD-Eintrag
- ord-3113dcc3f4d843929e0e8df71d5a0bf6
- Quelldatensatz
- uspto-grants-2016_05
- DOI