HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Anhydride → N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-5-(2-acetoxyethylthio)pentanamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | N-[4-(4-piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-5-(2-hydroxyethylthio)pentanamide | HCID 67725636 | — |
| Produkt | N-[4-(4-Piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-5-(2-acetoxyethylthio)pentanamide | HCID 67726287 | 92% |
Reaktionsschritte
Following a procedure similar to that described in Example 67(c), but using N-[4-(4-piperidinomethyl-2-pyridyloxy)-cis-2-butenyl]-5-(2-hydroxyethylthio)pentanamide [prepared as described in step (c) above] and acetic anhydride as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as an oil in a 92% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05616579 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-0cbd77638f9f47458ca28608a83435df |
| Quellennotiz | uspto-grants-1997_04 |