2-Propylhept-2-enal → 2-Propylheptanal

HRID 522251

Reaktionsgleichung

Reaktionsgleichung von HRID 522251
[CH2:1]([C:4](=[CH:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH:5]=[O:6])[CH2:2][CH3:3]>[Pd].[C]>[CH2:1]([CH:4]([CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH:5]=[O:6])[CH2:2][CH3:3]

Komponenten

3

Edukt 1

HCID 1187452-Propylhept-2-enal

Produkt 1

HCID 30186342-PropylheptanalAusbeute 97,8 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 178418390HCID 178418390, VerbindungKatalysator

Reaktionsbedingungen

Temperatur
75 °C

Versuchsvorschrift

An autoclave was charged with 420 g of 2-propyl-2-heptenal and 4 g of a 5% Pd carbon powder (water content: 56%, manufactured by N.E. Chemcat Corporation), and the mixture was stirred at 75° C. for 1.5 hours under a hydrogen pressure of 1.5 MPa. The reaction product was filtered through a membrane filter (PTFE, 0.5 μm) to obtain 416 g of 2-propylheptanal.

Aufarbeitung

  1. filtrationThe reaction product was filtered through a membrane
  2. filtrationfilter (PTFE, 0.5 μm)

Quellen und Nachweise

ORD-Eintrag
ord-f577967a37614483969cbe2e27e6788d
Quelldatensatz
uspto-grants-2016_05
Patentnummer
US09328306B2

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