Potassium Carbonate → S 20928

HRID 52289

Reaktionsgleichung

Reaktionsgleichung von HRID 52289
Cl.[C:2]1([CH2:12][CH2:13][NH2:14])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1.C(=O)([O-])[O-].[K+].[K+].[CH:21]1([C:25](Cl)=[O:26])[CH2:24][CH2:23][CH2:22]1>O.C(Cl)(Cl)Cl>[C:2]1([CH2:12][CH2:13][NH:14][C:25]([CH:21]2[CH2:24][CH2:23][CH2:22]2)=[O:26])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[CH:4][CH:3]=1

Komponenten

5

Edukt 3

HCID 11430Potassium CarbonateHCID 78705Cyclobutanecarbonyl chlorideHCID 123704372-(1-Naphthyl)ethylamine hydrochloride

Produkt 1

HCID 127856S 20928

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 22418719Chloroform waterLösungsmittel

Versuchsvorschrift

0.01 mol of N-[2-(1-naphthyl)ethyl]amine hydrochloride is dissolved in a water/chloroform (40: 60; vol/vol ) mixture, and 0.02 mol of potassium carbonate is then added with magnetic stirring. The reaction mixture is cooled in an ice bath, and 0.01 mol of cyclobutanecarbonyl chloride is then added dropwise with magnetic stirring.

Aufarbeitung

  1. additionis then added with magnetic stirring
  2. temperatureThe reaction mixture is cooled in an ice bath

Quellen und Nachweise

ORD-Eintrag
ord-8e4b4b7fd8854a2684e0c0c78407b175
Quelldatensatz
uspto-grants-1997_04
Patentnummer
US05616614

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