Benzoyl chloride → HCID 19963672, Verbindung

HRID 52437Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 52437
[CH2:1]([CH2:7][C:8]([NH2:10])=[S:9])[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1.[C:11](Cl)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(OCC)(=O)C>N1C=CC=CC=1>[C:11]([NH:10][C:8](=[S:9])[CH2:7][CH2:1][C:2]1[O:6][CH:5]=[CH:4][CH:3]=1)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Komponenten

5

Edukt 3

HCID 7412Benzoyl chlorideHCID 8857Ethyl AcetateHCID 199636792-Furfurylthioacetamide

Produkt 1

HCID 19963672HCID 19963672, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1049PyridineLösungsmittel

Reaktionsbedingungen

Temperatur
60 °C

Versuchsvorschrift

12.11 g (0.07 mol) of 2-furfurylthioacetamide was dissolved in 30 ml of pyridine. To the above solution, 9.94 g (0.07 mol) of benzoylchloride was added, and the mixture was stirred at 60° C. for 15 hours. The solvent was distilled away from the reaction mixture, and a residue thus obtained was added to ethyl acetate and washed successively with water twice, 1N hydrochloric acid, water three times, and brine. A resultant organic extract layer was dried, and the solvent was distilled away therefrom.

Aufarbeitung

  1. distillationThe solvent was distilled away from the reaction mixture
  2. customa residue thus obtained
  3. washwashed successively with water twice
  4. customA resultant organic extract layer was dried
  5. distillationthe solvent was distilled away

Quellen und Nachweise

ORD-Eintrag
ord-8daf3d01e7a4411b93e67d7293813538
Quelldatensatz
uspto-grants-1997_04
Patentnummer
US05616711

Notizen zur Reaktion

Wird geladen…