Ammonia → Morpholine-3-carboxamide
Reaktionsgleichung
Cl.[NH:2]1[CH2:7][CH2:6][O:5][CH2:4][CH:3]1[C:8]([O:10]C)=O.[NH3:12]>CO>[NH:2]1[CH2:7][CH2:6][O:5][CH2:4][CH:3]1[C:8]([NH2:12])=[O:10]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A mixture of methyl morpholine-3-carboxylate hydrochloride (0.55 g, 3.0 mmol) and a solution of NH3 in methanol (7 mol/L, 20 mL) was stirred at 50° C. for 24 hours in a sealed tube. The mixture was concentrated in vacuo to give the title compound as glutinous semisolid (0.39 g, 99%). The compound was characterized by the following spectroscopic data:
Aufarbeitung
- concentrationThe mixture was concentrated in vacuo
Quellen und Nachweise
- ORD-Eintrag
- ord-13e5a44e7f7c4fccb815db4929082891
- Quelldatensatz
- uspto-grants-2016_05
- Patentnummer
- US09340538B2
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