HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Morpholine-3-carboxamide → HCID 73294949, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Morpholine-3-carboxamide | HCID 19792002 | — |
| Edukt | Ethyl 6-(bromomethyl)-4-(2,4-dichlorophenyl)-2-(thiazol-2-yl)-1,4-dihydropyrimidine-5-carboxylate | HCID 118107510 | — |
| Produkt | HCID 73294949 | HCID 73294949 | 49% |
Reaktionsschritte
Ethyl 6-(bromomethyl)-4-(2,4-dichlorophenyl)-2-(thiazol-2-yl)-1,4-dihydropyrimidine-5-carboxylate (2.85 g, 6 mmol) was reacted with morpholine-3-carboxamide (0.78 g, 6 mmol) according to the procedure as described in Example 25, Step B to give the title compound as a yellow solid (1.54 g, 49%). The compound was characterized by the following spectroscopic data:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09340538B2 |
| Quelldatensatz | uspto-grants-2016_05 |
| ORD ID | ord-004aecd12c014c4e9bb133c6582e3fe3 |
| Quellennotiz | uspto-grants-2016_05 |