Sodium Hydroxide → 4-Methylpiperazine-2-carboxylic acid

HRID 524780Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 524780
[CH3:1][N:2]1[CH2:7][CH2:6][NH:5][CH:4]([C:8]([O:10]CC)=[O:9])[CH2:3]1.[OH-].[Na+]>>[CH3:1][N:2]1[CH2:7][CH2:6][NH:5][CH:4]([C:8]([OH:10])=[O:9])[CH2:3]1

Komponenten

3

Edukt 2

HCID 14798Sodium HydroxideHCID 12558522Ethyl 4-methylpiperazine-2-carboxylate

Produkt 1

HCID 64209034-Methylpiperazine-2-carboxylic acidAusbeute 100 %

Versuchsvorschrift

Ethyl 4-methylpiperazine-2-carboxylate (1.03 g, 6 mmol) was reacted with NaOH (0.48 g, 12 mmol) according to the procedure as described in Example 21, Step A to give the title compound as colorless oil (0.86 g, 100%). The compound was characterized by the following spectroscopic data:

Quellen und Nachweise

ORD-Eintrag
ord-88397e1baa204780b98e954df8ed3c75
Quelldatensatz
uspto-grants-2016_05
Patentnummer
US09340538B2

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