HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonium Chloride → 6-Methoxybenzo[d]thiazole-2-carboximidamide hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonium Chloride | HCID 25517 | — |
| Edukt | 2-Cyano-6-methoxy benzothiazole | HCID 342109 | — |
| Edukt | Sodium Methoxide | HCID 10942334 | — |
| Produkt | 6-Methoxybenzo[d]thiazole-2-carboximidamide hydrochloride | HCID 118107613 | 75% |
Reaktionsschritte
6-methoxybenzo[d]thiazole-2-carbonitrile (1 g, 5.26 mmol) was reacted with sodium methoxide (0.28 g, 5.26 mmol) and ammonium chloride (0.6 g, 11 mmol) according to the procedure as described in Example 61, Step B to give the title compound as a white solid (0.96 g, 75%). The compound was characterized by the following spectroscopic data:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09340538B2 |
| Quelldatensatz | uspto-grants-2016_05 |
| ORD ID | ord-a5da7ede6b604060ad6e1da9b0089605 |
| Quellennotiz | uspto-grants-2016_05 |