HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Anhydride → (R)-N2-Acetyl-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | (R)-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl)-ornithinamide | HCID 136381090 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | (R)-N2-Acetyl-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide | HCID 136381103 | — |
Reaktionsbedingungen
| Temperatur | 50 °C |
|---|
Reaktionsschritte
0.3 g (0.925 mMol) of (R)-N5 -[amino(nitroimino) methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide were dissolved in 3 ml of glacial acetic acid and after the addition of 3 ml (0.032 Mol) of acetic anhydride the mixture was heated to a reaction temperature of 50° C. for 30 minutes. The product remaining after the volatile components had evaporated off was further processed without purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05616620 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-32448bb5a54f41b6969b78bc6789bb71 |
| Quellennotiz | uspto-grants-1997_04 |