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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 52684Erstellt: 24. Oktober 2026

3,3,3-Trifluoropropene → 3,3,3-Trifluoropropylcyclopentyldiethoxysilane

https://huagongshe.com/de/reaction/52684

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3,3,3-TrifluoropropeneHCID 12672—
EduktCyclopentyldiethoxysilaneHCID 123987211—
KatalysatorIridium trichloride hydrateHCID 16211477—
LösungsmittelP-XyleneHCID 7809—
Produkt3,3,3-TrifluoropropylcyclopentyldiethoxysilaneHCID 2237767877%

Reaktionsschritte

In analogy to Example 3, a mixture of 3 g of p-xylene, 5.3 g (0.055 mol) of 3,3,3-trifluoro-1-propene and 9.4 g (0.5 mol) of cyclopentyldiethoxysilane was reacted in the presence of 0.1 mg of iridium(III) chloride hydrate, after a mixing time of 70 minutes, at 83° C. over 180 minutes. Analysis by gas chromatography gave a product yield of 77% of 3,3,3-trifluoropropylcyclopentyldiethoxysilane.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05616762
Quelldatensatzuspto-grants-1997_04
ORD IDord-844fb9cc8acf4c52b30fdadb2a3243f0
Quellennotizuspto-grants-1997_04