HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethoxysilane → Triethoxy(3-isocyanatopropyl)silane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethoxysilane | HCID 13830 | — |
| Edukt | Allyl isocyanate | HCID 15123 | — |
| Lösungsmittel | P-Xylene | HCID 7809 | — |
| Produkt | Triethoxy(3-isocyanatopropyl)silane | HCID 90613 | 71,8% |
Reaktionsschritte
In analogy to Example 6, a reaction mixture consisting of 640 g of p-xylene, 680 g (8.17 mol) of allyl isocyanate and 1250 g (7.6 mol) of triethoxysilane was reacted at from 76° to 92° C. over the course of 150 minutes. Working up by distillation gave 1350 g of 3-isocyanatopropyltriethoxysilane in addition to the trimer.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05616762 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-a6b7d28bd66448d9ab588797d7716d9f |
| Quellennotiz | uspto-grants-1997_04 |