Chloroacetic Acid → HCID 86750633, Verbindung
Reaktionsgleichung
S([CH2:5][C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34])=[O:7])(O)(=O)=O.[Na].[Cl:36]CC(O)=O>>[Cl:36][CH2:5][C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH3:34])=[O:7]Komponenten
3
Reaktionsbedingungen
- Temperatur
- 93 °C
Versuchsvorschrift
The reactor is then heated to a temperature of 93° C. and maintained at a temperature of between 90° C. and 97° C. for about 11 hours. HPLC analysis of the resulting slurry indicates that the sodium lauryl-myristyl sulfoacetate is substantially free of monochloroacetic acid and its salts.
Aufarbeitung
- temperaturemaintained at a temperature of between 90° C. and 97° C. for about 11 hours