HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl (chloroformyl)acetate → Ethyl thiazole-5-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl (chloroformyl)acetate | HCID 118030 | — |
| Edukt | Methanethioamide | HCID 3005587 | — |
| Produkt | Ethyl thiazole-5-carboxylate | HCID 459108 | 33% |
Reaktionsschritte
According to the procedure of Mashraqui and Keehn (J. Am. Chem. Soc. 1982, 104, 4461), ethyl α-chloro-α-formylacetate was condensed with thioformamide and vacuum distilled to provide 5.65 g (33%) of the desired compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05616714 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-f3518c71ebc14df68b241e1171fe4697 |
| Quellennotiz | uspto-grants-1997_04 |