Benzylamine → HCID 118201132, Verbindung
Reaktionsgleichung
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:9]1([CH2:13][CH:14]=O)[CH2:12][CH2:11][CH2:10]1>C(Cl)Cl>[CH:9]1([CH2:13][CH:14]=[N:8][CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH2:12][CH2:11][CH2:10]1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
Benzylamine (2.95 g, 27.5 mmol) was added to a mixture of cyclobutylacetaldehyde (30.6 mmol) in CH2Cl2 (˜238 mL) and molecular sieves (5.0 g) and the mixture was stirred at room temperature for 5.5 hours. The mixture was filtered over Celite and the solvent was removed under vacuum to yield 5.45 g of crude N-(2-cyclobutylethylidene)-1-phenylmethanamine.
Aufarbeitung
- filtrationThe mixture was filtered over Celite
- customthe solvent was removed under vacuum
Quellen und Nachweise
- ORD-Eintrag
- ord-68fd615743254ce5821775dd2ee41d1b
- Quelldatensatz
- uspto-grants-2016_05
- Patentnummer
- US09346853B2
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