Cyclohexylamine → Benzamide, N-[(cyclohexylamino)thioxomethyl]-

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

Benzoyl isothiocyanate (19.4 g, 118.9 mmol) was dissolved in dichloromethane and cooled to 0° C. Cyclohexylamine (13 g, 131.1 mmol) was added dropwise. Then the reaction was stirred at room temperature for 2 h. The mixture was washed with water, dried over sodium sulfate. Concentration under vaccum gave the title compound as a pale white solid in quantitative yield.

Herkunft & Nachweise