Methanol → 3-Methoxy-3-oxo-2-phenylpropanoic acid

HRID 53196

Reaktionsgleichung

Reaktionsgleichung von HRID 53196
[C:1]1([CH:7]([C:11]([OH:13])=[O:12])[C:8]([OH:10])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.B(F)(F)F.[CH3:18]COCC.CO>>[C:1]1([CH:7]([C:11]([OH:13])=[O:12])[C:8]([O:10][CH3:18])=[O:9])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Komponenten

4

Edukt 3

HCID 887MethanolHCID 8000Boron trifluoride etherateHCID 75791Phenylmalonic acid

Produkt 1

HCID 28177753-Methoxy-3-oxo-2-phenylpropanoic acid

Versuchsvorschrift

A mixture of phenylmalonic acid (3.6 g, 0.02 mol), boron trifluoride etherate (2.4 mL, 0.02 mol) and 0.8 mL of anhydrous methanol (0.02 mol) was refluxed and stirred for 24 hours. After cooling to room temperature, the reaction mixture was filtered and 20 mL of water was added.

Aufarbeitung

  1. temperaturewas refluxed
  2. filtrationthe reaction mixture was filtered
  3. addition20 mL of water was added

Quellen und Nachweise

ORD-Eintrag
ord-f0626949f0464962af6e6c41c959ad1b
Quelldatensatz
uspto-grants-1997_04
Patentnummer
US05618826

Verknüpfte Notizen

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