Urethane acrylate → 1-Hydroxycyclohexyl phenyl ketone

HRID 532095

Reaktionsgleichung

Reaktionsgleichung von HRID 532095
[C:1]([OH:5])(=O)[CH:2]=[CH2:3].[C:6]([OH:10])(=O)[CH:7]=[CH2:8].[C:11](O)(=O)[CH:12]=[CH2:13].[C:16](O)(=O)[CH:17]=[CH2:18].[C:21](O)(=O)C=C.C(O)(=O)C=C.OCC(CO)(CO)CO.C(O)(=O)C=C.NC(OCC)=O.C1(=O)OCCCCC1.OCC(CO)(COCC(CO)(CO)CO)CO>C(O)(C)C>[CH2:11]1[CH2:8][CH2:7][C:6]([OH:10])([C:1]([C:2]2[CH:3]=[CH:21][CH:16]=[CH:17][CH:18]=2)=[O:5])[CH2:13][CH2:12]1

Komponenten

5

Edukt 3

HCID 21863578Urethane acrylateHCID 66608674Dipentaerythritol caprolactoneHCID 131731916Pentaerythritol hexaacrylate

Produkt 1

HCID 703551-Hydroxycyclohexyl phenyl ketone

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 3776IsopropanolLösungsmittel

Versuchsvorschrift

A protective layer coating solution was prepared by mixing 3 parts by mass of pentaerythritol hexaacrylate (KAYARAD DPHA, produced by Nippon Kayaku Co., Ltd.), 3 parts by mass of an urethane acrylate oligomer (ART RESIN UN-3320HA, produced by Negami Chemical Industrial Co., Ltd.), 3 parts by mass of an acrylic acid ester of dipentaerythritol caprolactone (KAYARAD DPCA-120, produced by Nippon Kayaku Co., Ltd.), 1 part by mass of a silica (P-526, produced by Mizusawa Industrial Chemicals, Ltd.), 0.5 parts by mass of a photopolymerization initiator (IRGACURE 184, produced by Nihon Ciba-Geigy K.K.), and 11 parts by mass of isopropyl alcohol, and sufficiently agitating and dispersing the mixture with the use of a ball mill, such that the average particle diameter became approximately 3 μm.

Aufarbeitung

  1. customA protective layer coating solution was prepared

Quellen und Nachweise

ORD-Eintrag
ord-8b9d069eb1fd492a9b508b48fd643f04
Quelldatensatz
uspto-grants-2014_10
Patentnummer
US08852856B2

Verknüpfte Notizen

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