Benzamide → HCID 21192648, Verbindung

HRID 532379Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 532379
[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12])[C:5]([OH:7])=O.[C:15](N)(=O)C1C=CC=CC=1>>[Cl:1][C:2]1[CH:3]=[C:4]([C:5](=[O:7])[CH3:15])[CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12]

Komponenten

3

Edukt 2

HCID 2331BenzamideHCID 2400533-Chloro-4,5-dimethoxybenzoic acid

Produkt 1

HCID 21192648HCID 21192648, Verbindung

Versuchsvorschrift

3-Chloro-4,5-dimethoxybenzoic acid (1 g) was converted to the benzamide derivative analogously to O3.043, and the latter to the title compound analogously to O2.059. 495 mg of the title compound were obtained. LC-MS rt: 1.55 min [M+H]+: 215.1 (met. a)

Quellen und Nachweise

ORD-Eintrag
ord-514645e736e94448a038afcb55938c14
Quelldatensatz
uspto-grants-2014_10
Patentnummer
US08853206B2

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