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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 533235Erstellt: 23. Oktober 2026

Water → HCID 67316267, Verbindung

https://huagongshe.com/de/reaction/533235

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktWaterHCID 962—
EduktPotassium CarbonateHCID 11430—
Edukt1-NaphthalenethiolHCID 68259—
EduktHCID 87353567HCID 87353567—
LösungsmittelAcetonitrileHCID 6342—
ProduktHCID 67316267HCID 67316267—

Reaktionsschritte

A mixture of EXAMPLE 10A (42 mg), naphthalene thiol (45 mg), and potassium carbonate (36 mg) in acetonitrile (2 mL) was heated at 80° C. for 3 days. The reaction mixture was poured into water, extracted with dichloromethane and purified by flash chromatography on silica gel with 0-20% ethyl acetate in hexanes.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08853209B2
Quelldatensatzuspto-grants-2014_10
ORD IDord-e1dfa09626a14fc0925b8340aa0a84fc
Quellennotizuspto-grants-2014_10