2-Bromo-1-(3-chloro-5-(trifluoromethyl)phenyl)ethanone → 2-Bromo-1-(3-bromo-5-(trifluoromethyl)phenyl)ethanone

HRID 534849Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 534849
[Br:1][C:2]1[CH:3]=[C:4]([C:12](=[O:14])[CH3:13])[CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.[Br:15]CC(C1C=C(C(F)(F)F)C=C(Cl)C=1)=O>>[Br:15][CH2:13][C:12]([C:4]1[CH:5]=[C:6]([C:8]([F:10])([F:11])[F:9])[CH:7]=[C:2]([Br:1])[CH:3]=1)=[O:14]

Komponenten

3

Edukt 2

HCID 197023082-Bromo-1-(3-chloro-5-(trifluoromethyl)phenyl)ethanoneHCID 218526683'-Bromo-5'-(trifluoromethyl)acetophenone

Produkt 1

HCID 197023342-Bromo-1-(3-bromo-5-(trifluoromethyl)phenyl)ethanoneAusbeute 99 %

Versuchsvorschrift

The title compound was prepared from 1-(3-bromo-5-(trifluoromethyl)phenyl)ethanone (Reference Example 41) by a procedure similar to the one described for 2-bromo-1-(3-chloro-5-(trifluoromethyl)phenyl)ethanone (Reference Example 34) to provide 2-bromo-1-(3-bromo-5-(trifluoromethyl)phenyl)ethanone (23.17 g, >99%) as a yellow oil.

Quellen und Nachweise

ORD-Eintrag
ord-ae0cc16da852482db166ccc4a6fec3c7
Quelldatensatz
uspto-grants-2014_10
Patentnummer
US08853215B2

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