HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanolamine → Dipyridodiazepinone deriv. 23
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanolamine | HCID 700 | — |
| Edukt | Dipyridodiazepinone deriv. 15 | HCID 463144 | — |
| Produkt | Dipyridodiazepinone deriv. 23 | HCID 463150 | — |
Reaktionsschritte
The title compound, m.p. 241°-244° C., was synthesized from 2-chloro-5,11-dihydro-11-ethyl-4-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and ethanolamine using procedures analogous to those described above, except that the mixture was heated in a pressure bottle at 260° C. for 50 min., and the product was crystallized from chloroform/ethanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05620974 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-188b5b5854db42b897e43c3abfb0c01f |
| Quellennotiz | uspto-grants-1997_04 |