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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 53548Erstellt: 23. Oktober 2026

Ethanolamine → Dipyridodiazepinone deriv. 23

https://huagongshe.com/de/reaction/53548

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanolamineHCID 700—
EduktDipyridodiazepinone deriv. 15HCID 463144—
ProduktDipyridodiazepinone deriv. 23HCID 463150—

Reaktionsschritte

The title compound, m.p. 241°-244° C., was synthesized from 2-chloro-5,11-dihydro-11-ethyl-4-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and ethanolamine using procedures analogous to those described above, except that the mixture was heated in a pressure bottle at 260° C. for 50 min., and the product was crystallized from chloroform/ethanol.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05620974
Quelldatensatzuspto-grants-1997_04
ORD IDord-188b5b5854db42b897e43c3abfb0c01f
Quellennotizuspto-grants-1997_04