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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 53549Erstellt: 23. Oktober 2026

N-(2-Aminoethyl)ethyleneurea → 5,11-Dihydro-11-ethyl-2-(2-imidazolon-1-yl)ethylamino-4-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one

https://huagongshe.com/de/reaction/53549

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN-(2-Aminoethyl)ethyleneureaHCID 80480—
EduktDipyridodiazepinone deriv. 15HCID 463144—
Produkt5,11-Dihydro-11-ethyl-2-(2-imidazolon-1-yl)ethylamino-4-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-oneHCID 86748265—

Reaktionsschritte

The title compound, m.p.>300° C., was synthesized from 2-chloro-5,11-dihydro-11-ethyl-4-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and 1-(2-aminoethyl)-2-imidazolidone using procedures analogous to those described above, except that the mixture was heated in a pressure bottle at 250° C. for 30 min., and the product was crystallized from acetic acid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05620974
Quelldatensatzuspto-grants-1997_04
ORD IDord-8f728ddb2d0a4c8fbb4885f5e2e57f70
Quellennotizuspto-grants-1997_04