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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 53550Erstellt: 23. Oktober 2026

3-Amino-1-propanol → Dipyridodiazepinone deriv. 24

https://huagongshe.com/de/reaction/53550

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt3-Amino-1-propanolHCID 9086—
EduktDipyridodiazepinone deriv. 15HCID 463144—
ProduktDipyridodiazepinone deriv. 24HCID 463151—

Reaktionsschritte

The title compound, m.p. 222°-224° C., was synthesized from 2-chloro-5,11-dihydro-11-ethyl-4-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and 3-aminopropanol using procedures analogous to those described above, except that the mixture was heated in a pressure bottle at 210° C. for 40 min., and the product was crystallized from ethyl acetate.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05620974
Quelldatensatzuspto-grants-1997_04
ORD IDord-5844411c24cd4bec8e690adcbf227b5e
Quellennotizuspto-grants-1997_04