HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
L-Valine → 2-[2-[2-(1-Carboxy-2-methylpropylcarbamoyl) phenyldisulfanyl]benzoylamino]-3-methylbutanoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | L-Valine | HCID 6287 | — |
| Edukt | 2,2'-Dithiodibenzoyl chloride | HCID 88164 | — |
| Produkt | 2-[2-[2-(1-Carboxy-2-methylpropylcarbamoyl) phenyldisulfanyl]benzoylamino]-3-methylbutanoic acid | HCID 465364 | — |
Reaktionsschritte
Using the method employed in Preparation 30, 17.8 g (0.15 mol) of D,L valine was reacted with 17.2 g (0.05 mol) of 2,2'-dithiobisbenzoyl chloride to produce 11.4 g of the title compound after recrystallization from acetic acid, mp 226.5°-227.5° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05620997 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-6384edd1f37f4d659d1d749143aaebcc |
| Quellennotiz | uspto-grants-1997_04 |