HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Butanal → Methyl 4-(1-hydroxybutyl)-3-methylbenzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Butanal | HCID 261 | — |
| Edukt | Methyl 4-Iodo-3-methylbenzoate | HCID 231757 | — |
| Produkt | Methyl 4-(1-hydroxybutyl)-3-methylbenzoate | HCID 68178586 | — |
Reaktionsschritte
The title compound was prepared by a method analogous to that described for Intermediate (16), using methyl 4-iodo-3-methylbenzoate and butyraldehyde. 1H NMR (400 MHz, CDCl3, δ): 7.87 (d, J=8.4 Hz, 1H), 7.81 (s, 1H), 7.56 (d, J=8.4 Hz, 1H), 4.98 (q, J=4.4 Hz, 1H), 3.90 (s, 3H), 2.37 (s, 3H), 1.63-1.72 (m, 2H), 1.50-1.54 (m, 1H), 1.39-1.43 (m, 1H), 0.98 (t, J=7.6 Hz, 3H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08859591B2 |
| Quelldatensatz | uspto-grants-2014_10 |
| ORD ID | ord-f933a18d40ce49698fd28bce0a78305c |
| Quellennotiz | uspto-grants-2014_10 |