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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 541177Erstellt: 26. Oktober 2026

4-Phenyl-2-butanol → 4-Methoxybenzyl alcohol

https://huagongshe.com/reaction/541177

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-Phenyl-2-butanolHCID 61302—
Eduktalpha-Methyl-2-pyridinemethanolHCID 86784—
Edukt2-Oxido-2-azoniatricyclo[3.3.1.03,7]nonaneHCID 101536640—
Produkt4-Methoxybenzyl alcoholHCID 7738—

Reaktionsschritte

2-(1-Hydroxyethyl)pyridine (76.8 mg, 0.624 mmol) was oxidized in the same manner as that described in Example 8, (a) (except that Nor-AZADO was used at 3 mol %, and the reaction was performed at room temperature) to obtain the objective compound (66.0 mg; yield, 87.4%). The spectrum data were found to be the same as those obtained in Example 6, (h).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08871981B2
Quelldatensatzuspto-grants-2014_10
ORD IDord-31220d8df9174332927d5f16647c901d
Quellennotizuspto-grants-2014_10