HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-methyl-1H-imidazole-2-carboxylic acid → HCID 86636212, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-methyl-1H-imidazole-2-carboxylic acid | HCID 557678 | — |
| Edukt | N-[6-chloro-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-yl]-2-piperidin-4-ylacetamide bis(trifluoroacetate) | HCID 86636208 | — |
| Produkt | HCID 86636212 | HCID 86636212 | 70% |
Reaktionsschritte
The desired compound was prepared according to the procedure of Example A27, using N-[6-chloro-2,4,8,18,22-pentaazatetracyclo[14.3.1.1(3,7).1(9,13)]docosa-1(20),3(22),4,6,9(21),10,12,16,18-nonaen-12-yl]-2-piperidin-4-ylacetamide bis(trifluoroacetate) and 1-methyl-1H-imidazole-2-carboxylic acid as starting materials in 70% yield. LCMS for C29H31ClN9O2 (M+H)+: m/z=572.2.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08871753B2 |
| Quelldatensatz | uspto-grants-2014_10 |
| ORD ID | ord-669e1b5bfb8d403581c42cb892006c5c |
| Quellennotiz | uspto-grants-2014_10 |