HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dacthal → HCID 70462314, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dacthal | HCID 2943 | — |
| Edukt | 7-Aminocephalosporanic acid | HCID 441328 | — |
| Edukt | HCID 178521532 | HCID 178521532 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | HCID 70462314 | HCID 70462314 | — |
Reaktionsschritte
While utilizing 0.680 g of 7-ACA, 0.900 g of 5-mercapto-2-morpholinocarbonylmethylthio-1,3,4-thiadiazole, 4.0 ml of acetonitrile and 2.70 g of DCPA, the procedure was carried out in accordance with Example 5, and there was obtained 1.02 g (83.3% of yield) of red brown powder of 7-amino-3-[(2-morpholinocarbonylmethylthio-1,3,4-thiadiazol-5-yl)thiomethyl]-3-cephem-4-carboxylic acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04446318 |
| Quelldatensatz | uspto-grants-1984_05 |
| ORD ID | ord-291c79c7964c4fc395677d94a85f454b |
| Quellennotiz | uspto-grants-1984_05 |