Methyl iodide → HCID 178504040, Verbindung

HRID 543794Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 543794
[F:1][C:2]([F:9])([F:8])[CH2:3][NH:4][C:5]([NH2:7])=[S:6].[CH3:10][I:11]>CCO>[IH:11].[F:1][C:2]([F:9])([F:8])[CH2:3][NH:4][C:5](=[NH:7])[S:6][CH3:10]

Komponenten

4

Edukt 2

HCID 6328Methyl iodideHCID 202028121-(2,2,2-Trifluoroethyl)thiourea

Produkt 1

HCID 178504040HCID 178504040, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

A solution of 2,2,2-trifluoroethylthiourea (8.0 g.) and methyl iodide (3.5 g.) in EtOH (40 ml.) was heated under reflux for 70 minutes, then evaporated to dryness in vacuo. The residue was triturated with ether to give 2,2,2-trifluoroethyl-S-methylisothiourea hydroiodide, m.p. 154°-156° (90%).

Aufarbeitung

  1. temperatureunder reflux for 70 minutes
  2. customevaporated to dryness in vacuo
  3. customThe residue was triturated with ether

Quellen und Nachweise

ORD-Eintrag
ord-eb664b0dcd9f44d985ecb0985c5b3da2
Quelldatensatz
uspto-grants-1984_05
Patentnummer
US04447441

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