HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-bromobutanimide → 2-(Bromomethyl)-3-chloro-1,1'-biphenyl
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-bromobutanimide | HCID 67184 | — |
| Edukt | 3-Chloro-2-methylbiphenyl | HCID 4601832 | — |
| Lösungsmittel | Carbon Tetrachloride | HCID 5943 | — |
| Produkt | 2-(Bromomethyl)-3-chloro-1,1'-biphenyl | HCID 13320700 | — |
Reaktionsschritte
A mixture of 3-chloro-2-methyl[1,1'-biphenyl] (10.4 grams, 0.051 mole) and N-bromosuccinimide (9.2 grams, 0.052 mole) in carbon tetrachloride (150 ml) was heated and irradiated with an infrared lamp for two hours. The mixture was cooled and filtered. The filtrate was evaporated under reduced pressure to give a quantitative yield of 2-bromomethyl-3-chloro[1,1'-biphenyl] as a yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04451484 |
| Quelldatensatz | uspto-grants-1984_05 |
| ORD ID | ord-c6f05b515ffa4cb4b7c949cce15d8276 |
| Quellennotiz | uspto-grants-1984_05 |