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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 544674Erstellt: 25. Oktober 2026

N-bromobutanimide → 2-(Bromomethyl)-3-chloro-1,1'-biphenyl

https://huagongshe.com/reaction/544674

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktN-bromobutanimideHCID 67184—
Edukt3-Chloro-2-methylbiphenylHCID 4601832—
LösungsmittelCarbon TetrachlorideHCID 5943—
Produkt2-(Bromomethyl)-3-chloro-1,1'-biphenylHCID 13320700—

Reaktionsschritte

A mixture of 3-chloro-2-methyl[1,1'-biphenyl] (10.4 grams, 0.051 mole) and N-bromosuccinimide (9.2 grams, 0.052 mole) in carbon tetrachloride (150 ml) was heated and irradiated with an infrared lamp for two hours. The mixture was cooled and filtered. The filtrate was evaporated under reduced pressure to give a quantitative yield of 2-bromomethyl-3-chloro[1,1'-biphenyl] as a yellow oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04451484
Quelldatensatzuspto-grants-1984_05
ORD IDord-c6f05b515ffa4cb4b7c949cce15d8276
Quellennotizuspto-grants-1984_05