2-Acetamidoacrylic acid → Methyl alpha-acetamidocinnamate

HRID 546332

Reaktionsgleichung

Reaktionsgleichung von HRID 546332
[C:1](NC(=C)C(O)=O)(=O)C.[C:10]([NH:13][C:14](=[CH:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:15]([OH:17])=[O:16])(=[O:12])[CH3:11].[Si](C=[N+]=[N-])(C)(C)C>>[C:10]([NH:13][C:14](=[CH:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:15]([O:17][CH3:1])=[O:16])(=[O:12])[CH3:11]

Komponenten

4

Edukt 3

HCID 794822-Acetamidoacrylic acidHCID 956312-(Acetylamino)-3-phenyl-2-propenoic acidHCID 167693Trimethylsilyldiazomethane

Produkt 1

HCID 340163Methyl alpha-acetamidocinnamate

Versuchsvorschrift

2-Acetamidoacrylic acid and acetamidocinnamic acid were hydrogenated using the same general procedure, derivatised using TMS-diazomethane and analysed using the same method described for the corresponding methyl esters.

Quellen und Nachweise

ORD-Eintrag
ord-5351a15de92f495fa9c21f56e7f0b790
Quelldatensatz
uspto-grants-2011_05
Patentnummer
US07935841B2

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