HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
TIBA isododecane → 2,3,5-Triiodobenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | TIBA isododecane | HCID 131728349 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 2,3,5-Triiodobenzoic acid | HCID 6948 | — |
Reaktionsschritte
33.3 ml of TIBA/isododecane solution (101 g/L) was mixed with 7.9 cc of MAO/toluene solution (Albemarle −30% wt) to obtain a MAO/TIBA molar ratio of 2:1. The solution was stirred for 1 hour at room temperature. Then, 69 mg of A-1 was dissolved in the solution.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07943716B2 |
| Quelldatensatz | uspto-grants-2011_05 |
| ORD ID | ord-7c8ef107c3634e86a66b5e20aa7b8cba |
| Quellennotiz | uspto-grants-2011_05 |