HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium hydride → HCID 53958130, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | Thiophene-3-methanol | HCID 123570 | — |
| Edukt | 2,6-Dichloro-4-(methylthio)pyridine | HCID 18950231 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | HCID 53958130 | HCID 53958130 | — |
Reaktionsschritte
To a solution containing 3-thiophenemethanol (0.56 g, 0.0041×1.2 mol) and sodium hydride (0.17 g, (ca.60% in mineral oil), 0.0041×1.05 mol) in tetrahydrofuran, 2,6- dichloro-4-methylmercaptopyridine (0.80 g, 0. 0041 mol) was added, and the resultant solution was refluxed for about 2 hours.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05624942 |
| Quelldatensatz | uspto-grants-1997_04 |
| ORD ID | ord-616d9f37c73c42489fa4cc1f958488ae |
| Quellennotiz | uspto-grants-1997_04 |