HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Bromoacetonitrile → [4-(2-Ethoxy-ethyl)-piperazin-1-yl]-acetonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Bromoacetonitrile | HCID 11534 | — |
| Edukt | 1-(2-Ethoxyethyl)piperazine | HCID 2734643 | — |
| Produkt | [4-(2-Ethoxy-ethyl)-piperazin-1-yl]-acetonitrile | HCID 63336683 | — |
Reaktionsschritte
The title compound is synthesized by coupling of 4-(2-Ethoxy-ethyl)-piperazine (commercially available from ABCR GmbH) and bromoacetonitrile analogously to the preparation of Intermediate 149.2 as a colorless oil; ES-MS: M+H=198.2; 1HNMR(DMSO-d6) 3.70 (s, 2H), 3.45 (q, 2H), 3.40 (q, 2H), 2.40-2.30 (m, 10H), 1.05 (t, 3H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08053457B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-50ac3cb6e71e44babcad2700b39d0b9f |
| Quellennotiz | uspto-grants-2011_11 |