HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl iodide → 3-Methoxy-2-nitropyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 3-Hydroxy-2-nitropyridine | HCID 27057 | — |
| Produkt | 3-Methoxy-2-nitropyridine | HCID 556063 | 97,4% |
Reaktionsschritte
The similar reaction as described in Reference Example 9 by using 2-nitro-3-hydroxypyridine (7.0 g), potassium carbonate (6.91 g) and methyl iodide (4.67 ml) gave the title compound (7.5 g) as crystalline powders.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08058280B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-756d09c03e2646658d6e0c70c3ed0126 |
| Quellennotiz | uspto-grants-2011_11 |