HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Chlorobenzaldehyde → HCID 11647370, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Edukt | Acetic acid, 2,2'-[methylenebis(sulfonyl)]bis- | HCID 2252641 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | HCID 11647370 | HCID 11647370 | 80% |
Reaktionsschritte
A solution of 4-chlorobenzaldehyde (2 mmol) and carboxymethane-sulfonylmethanesulfonyl-acetic acid (1 mmol) in acetic acid (10 mL) was subjected to General Procedure 1, to yield the title compound in 80% yield. m.p. 178-180° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08058313B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-8abc80da4f8e4c3c84a95e9311ea157b |
| Quellennotiz | uspto-grants-2011_11 |