HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl iodide → 5-Fluoro-2,3-dimethyl-benzothiazol-3-ium iodide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | 5-Fluoro-2-methylbenzothiazole | HCID 597437 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 5-Fluoro-2,3-dimethyl-benzothiazol-3-ium iodide | HCID 66990784 | — |
Reaktionsschritte
13.0 g (10.4 ml, 77.7 mmol) 5-Fluoro-2-methyl-benzothiazole and 22.1 g (9.47 ml, 156 mmol) iodomethane were boiled in ethanol for 7 h. The residue was filtrated. 4.00 g=17% white powder
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08058431B2 |
| Quelldatensatz | uspto-grants-2011_11 |
| ORD ID | ord-ca4303ac31c042c0bca4858ea5b4ad7a |
| Quellennotiz | uspto-grants-2011_11 |